Study on polymeric precursor pyrolysis synthesis and growth mechanism of Si3N4 nanobelts

Authors

    Authors

    Z. P. Xie; W. Y. Yang; H. T. Wang; G. Q. Liu; H. Z. Miao;A. Linan

    Comments

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    Abbreviated Journal Title

    Rare Metal Mat. Eng.

    Keywords

    polymeric precursor; pyrolysis; Si3N4 nanobelts; solid-liquid-gas-solid; growth mechanism; SINGLE; NANOWIRES; NANORODS; THIN; Materials Science, Multidisciplinary; Metallurgy & Metallurgical; Engineering

    Abstract

    A new method named catalyst-assisted pyrolysis of polymeric precursor to synthesize single-crystalline Si3N4 nanobelts was studied in this current paper. The process of the method contained three main steps such as cross-linking of polymeric precursor at a low temperature, high-energy ball milling and polymer pyrolysis at a high temperature. The as-synthesized nanobelts were detailed characterization by SEM, XRD, EDS, TEM and HRTEM. The growth mechanism for the single-crystalline Si3N4 nanobelts was proposed.

    Journal Title

    Rare Metal Materials and Engineering

    Volume

    36

    Publication Date

    1-1-2007

    Document Type

    Article

    Language

    Chinese

    First Page

    289

    Last Page

    292

    WOS Identifier

    WOS:000250915200083

    ISSN

    1002-185X

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